Keith, the problem may have been the inert binding material in the Campden. It doesn't dissolve well in bulk. I don't know how you add Campden, but years and years of doing this has taught me a few things. First, use a wine thief or siphon and draw out a cup of juice from the must. Strain it through a double layer of muslin if you have to. Then crush the Campden really good. It needs to be in a very fine powder, like powdered sugar. I use a glass mortar and pestle -- takes about 45 seconds once you get the technique down. If you just crush them with a spoon, bottle or something else, you're going to do a lot more work than with a mortar and pestle. Put the powdered Campden in a sanitized glass or jar and dump the juice in with it (add the liquid to the powder). Use a small whisk or a long-tined fork to whip the juice. In 30 seconds or so the Campden should be dissolved. Set it aside for a few minutes and then look at it. If any powder is evident as small bead-like clumps, whip it again. When all Campden is dissolved, stir this back into the must.
Jack Keller, The Winemaking Home Page
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